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Information card for entry 4081341
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Coordinates | 4081341.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Pd-complex |
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Chemical name | Pd-complex |
Formula | C56 H70 N4 O17 Pd2 |
Calculated formula | C57.81 H66 N4 O15 Pd2 |
Title of publication | Aerobic C‒H Acetoxylation of 8-Methylquinoline in PdII‒Pyridinecarboxylic Acid Systems: Some Structure‒Reactivity Relationships |
Authors of publication | Wang, Daoyong; Zavalij, Peter Y.; Vedernikov, Andrei N. |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 17 |
Pages of publication | 4882 |
a | 13.4534 ± 0.0017 Å |
b | 15.2917 ± 0.0019 Å |
c | 15.3176 ± 0.0019 Å |
α | 111.35 ± 0.0019° |
β | 92.9602 ± 0.0019° |
γ | 98.317 ± 0.002° |
Cell volume | 2885.4 ± 0.6 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0735 |
Residual factor for significantly intense reflections | 0.0599 |
Weighted residual factors for significantly intense reflections | 0.1226 |
Weighted residual factors for all reflections included in the refinement | 0.1274 |
Goodness-of-fit parameter for all reflections included in the refinement | 1 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4081341.html
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