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Information card for entry 4081386
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Coordinates | 4081386.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H56 Li4 N8 |
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Calculated formula | C28 H54.024 Li4 N8 |
Title of publication | 2-Aminopyrrolyl Dilithium Compounds: Synthesis, Structural Diversity, and Catalytic Activity for Amidation of Aldehydes with Amines |
Authors of publication | Guo, Zhiqiang; Liu, Qiao; Wei, Xuehong; Zhang, Yongbin; Tong, Hongbo; Chao, Jianbin; Guo, Jianping; Liu, Diansheng |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 16 |
Pages of publication | 4677 |
a | 9.816 ± 0.004 Å |
b | 10.545 ± 0.005 Å |
c | 17.265 ± 0.007 Å |
α | 90° |
β | 103.845 ± 0.009° |
γ | 90° |
Cell volume | 1735.2 ± 1.3 Å3 |
Cell temperature | 233 ± 2 K |
Ambient diffraction temperature | 233 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1017 |
Residual factor for significantly intense reflections | 0.0603 |
Weighted residual factors for significantly intense reflections | 0.1558 |
Weighted residual factors for all reflections included in the refinement | 0.1834 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.01 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4081386.html
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structural data.