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Information card for entry 4081408
Preview
Coordinates | 4081408.cif |
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Original paper (by DOI) | HTML |
Formula | C30 H34 N2 S3 Sn |
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Calculated formula | C30 H34 N2 S3 Sn |
SMILES | [Sn](Sc1ccccc1)(Sc1ccccc1)(Sc1ccccc1)c1c(CN(C)C)cccc1CN(C)C |
Title of publication | Reactivity of Organotin(I) Dimers RSnSnR (R = 2,6-(Me2NCH2)2C6H3, 4-t-Bu-2,6-{P(O)(O-i-Pr)2}2C6H2) with Diaryl Dichalcogenides, ArEEAr (E = S, Se, Te; Ar = Ph, 2-C5H4N): Control of Secondary Sn···Sn Interactions by Intramolecular Coordination and Identity of the Aryl Chalcogenate |
Authors of publication | Wagner, Michael; Dietz, Christina; Bouška, Marek; Dostál, Libor; Padĕlková, Zdeňka; Jambor, Roman; Jurkschat, Klaus |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 17 |
Pages of publication | 4973 |
a | 9.924 ± 0.0007 Å |
b | 10.634 ± 0.0013 Å |
c | 28.755 ± 0.003 Å |
α | 99.536 ± 0.008° |
β | 98.171 ± 0.006° |
γ | 97.784 ± 0.008° |
Cell volume | 2922.7 ± 0.5 Å3 |
Cell temperature | 150 ± 1 K |
Ambient diffraction temperature | 150 ± 1 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.076 |
Residual factor for significantly intense reflections | 0.049 |
Weighted residual factors for significantly intense reflections | 0.0801 |
Weighted residual factors for all reflections included in the refinement | 0.089 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.113 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4081408.html
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Users of the data should acknowledge the original authors of the
structural data.