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Information card for entry 4081413
Preview
Coordinates | 4081413.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | [1(P),3(Sn)-Sn(S-Py)2-OP(O)(O-i-Pr)-6-t-Bu-4-P(O)(Oi-Pr)2]C6H2 |
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Formula | C32 H46 N2 O6 P2 S2 Sn |
Calculated formula | C32 H46 N2 O6 P2 S2 Sn |
Title of publication | Reactivity of Organotin(I) Dimers RSnSnR (R = 2,6-(Me2NCH2)2C6H3, 4-t-Bu-2,6-{P(O)(O-i-Pr)2}2C6H2) with Diaryl Dichalcogenides, ArEEAr (E = S, Se, Te; Ar = Ph, 2-C5H4N): Control of Secondary Sn···Sn Interactions by Intramolecular Coordination and Identity of the Aryl Chalcogenate |
Authors of publication | Wagner, Michael; Dietz, Christina; Bouška, Marek; Dostál, Libor; Padĕlková, Zdeňka; Jambor, Roman; Jurkschat, Klaus |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 17 |
Pages of publication | 4973 |
a | 17.0979 ± 0.001 Å |
b | 11.334 ± 0.0007 Å |
c | 19.9926 ± 0.0013 Å |
α | 90° |
β | 113.008 ± 0.007° |
γ | 90° |
Cell volume | 3566.1 ± 0.4 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0558 |
Residual factor for significantly intense reflections | 0.031 |
Weighted residual factors for significantly intense reflections | 0.0575 |
Weighted residual factors for all reflections included in the refinement | 0.0597 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.807 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4081413.html
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Users of the data should acknowledge the original authors of the
structural data.