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Information card for entry 4081460
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Coordinates | 4081460.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | [K(2,2,2-crypt)][Zn(mes)(THF)(Et3Al:IPr-H)2] |
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Formula | C93 H147 Al2 K N6 O6 Zn |
Calculated formula | C93 H147 Al2 K N6 O6 Zn |
Title of publication | Group 12 Metal Complexes of N-Heterocyclic Ditopic Carbanionic Carbenes |
Authors of publication | Waters, Jordan B.; Turbervill, Robert S. P.; Goicoechea, Jose M. |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 18 |
Pages of publication | 5190 |
a | 23.0241 ± 0.0015 Å |
b | 37.2937 ± 0.0013 Å |
c | 11.0391 ± 0.0006 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 9478.8 ± 0.9 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 33 |
Hermann-Mauguin space group symbol | P n a 21 |
Hall space group symbol | P 2c -2n |
Residual factor for all reflections | 0.0749 |
Residual factor for significantly intense reflections | 0.0594 |
Weighted residual factors for significantly intense reflections | 0.1574 |
Weighted residual factors for all reflections included in the refinement | 0.169 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.043 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4081460.html
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