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Information card for entry 4081600
Preview
Coordinates | 4081600.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C46 H54 I3 N2 P2 Si2 Te |
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Calculated formula | C46 H54 I3 N2 P2 Si2 Te |
Title of publication | CH‒NH Tautomerism in the Products of the Reactions of the Methanide [HC(PPh2NSiMe3)2]−with Pnictogen and Tellurium Iodides |
Authors of publication | Thirumoorthi, Ramalingam; Chivers, Tristram; Gendy, Chris; Vargas-Baca, Ignacio |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 19 |
Pages of publication | 5360 |
a | 10.805 ± 0.0002 Å |
b | 13.055 ± 0.0002 Å |
c | 19.446 ± 0.0004 Å |
α | 80.973 ± 0.0009° |
β | 76.625 ± 0.0009° |
γ | 71.99 ± 0.001° |
Cell volume | 2527.05 ± 0.08 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0496 |
Residual factor for significantly intense reflections | 0.0398 |
Weighted residual factors for significantly intense reflections | 0.0756 |
Weighted residual factors for all reflections included in the refinement | 0.0813 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.108 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4081600.html
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