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Information card for entry 4081603
Preview
Coordinates | 4081603.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C31 H41 I3 N2 P2 Si2 Te |
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Calculated formula | C31 H41 I3 N2 P2 Si2 Te |
Title of publication | CH‒NH Tautomerism in the Products of the Reactions of the Methanide [HC(PPh2NSiMe3)2]−with Pnictogen and Tellurium Iodides |
Authors of publication | Thirumoorthi, Ramalingam; Chivers, Tristram; Gendy, Chris; Vargas-Baca, Ignacio |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 19 |
Pages of publication | 5360 |
a | 10.38 ± 0.005 Å |
b | 12.247 ± 0.005 Å |
c | 16.205 ± 0.005 Å |
α | 91.9 ± 0.005° |
β | 101.227 ± 0.005° |
γ | 104.26 ± 0.005° |
Cell volume | 1951.2 ± 1.4 Å3 |
Cell temperature | 123 ± 2 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0526 |
Residual factor for significantly intense reflections | 0.0426 |
Weighted residual factors for significantly intense reflections | 0.0801 |
Weighted residual factors for all reflections included in the refinement | 0.0858 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.102 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4081603.html
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