Information card for entry 4081674

Structure parameters

• Formula: C67 H88 N4 P2 Si Y
• Calculated formula: C67 H88 N4 P2 Si Y
• Title of publication: Facile Preparation of a Scandium Terminal Imido Complex Supported by a Phosphazene Ligand
• Authors of publication: Rong, Weifeng; Cheng, Jianhua; Mou, Zehuai; Xie, Hongyan; Cui, Dongmei
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 19
• Pages of publication: 5523
• a: 48.821 ± 0.003 Å
• b: 14.3262 ± 0.0008 Å
• c: 19.149 ± 0.0012 Å
• α: 90°
• β: 108.78 ± 0.001°
• γ: 90°
• Cell volume: 12680.2 ± 1.3 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1577
• Residual factor for significantly intense reflections: 0.0732
• Weighted residual factors for significantly intense reflections: 0.1589
• Weighted residual factors for all reflections included in the refinement: 0.1992
• Goodness-of-fit parameter for all reflections included in the refinement: 0.981
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No