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Information card for entry 4081694
Preview
Coordinates | 4081694.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C51 H54 N2 O Si W |
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Calculated formula | C51 H54 N2 O Si W |
SMILES | [W]1(CCC1)(=Nc1c(cccc1c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C)(n1c(ccc1C)C)O[Si](c1ccccc1)(c1ccccc1)c1ccccc1 |
Title of publication | Synthesis of Methylidene Complexes that Contain a 2,6-Dimesitylphenylimido Ligand and Ethenolysis of 2,3-Dicarbomethoxynorbornadiene |
Authors of publication | Gerber, Laura C. H.; Schrock, Richard R. |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 19 |
Pages of publication | 5573 |
a | 19.6235 ± 0.0016 Å |
b | 22.9245 ± 0.0019 Å |
c | 19.7261 ± 0.0017 Å |
α | 90° |
β | 91.756 ± 0.002° |
γ | 90° |
Cell volume | 8869.8 ± 1.3 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0421 |
Residual factor for significantly intense reflections | 0.022 |
Weighted residual factors for significantly intense reflections | 0.0494 |
Weighted residual factors for all reflections included in the refinement | 0.0596 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4081694.html
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