Information card for entry 4081696

Structure parameters

• Formula: C70.94 H85.3 N4.53 O6.47 Si W
• Calculated formula: C70.944 H85.304 N4.528 O6.472 Si W
• Title of publication: Synthesis of Methylidene Complexes that Contain a 2,6-Dimesitylphenylimido Ligand and Ethenolysis of 2,3-Dicarbomethoxynorbornadiene
• Authors of publication: Gerber, Laura C. H.; Schrock, Richard R.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 19
• Pages of publication: 5573
• a: 12.0776 ± 0.0007 Å
• b: 12.8509 ± 0.0007 Å
• c: 22.2515 ± 0.0013 Å
• α: 88.694 ± 0.001°
• β: 83.724 ± 0.001°
• γ: 75.045 ± 0.001°
• Cell volume: 3316.6 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0423
• Residual factor for significantly intense reflections: 0.0375
• Weighted residual factors for significantly intense reflections: 0.087
• Weighted residual factors for all reflections included in the refinement: 0.0887
• Goodness-of-fit parameter for all reflections included in the refinement: 1.274
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No