Information card for entry 4081716

Structure parameters

• Formula: C42 H42 B Cl Ge O1.5 P2
• Calculated formula: C42 H38 B Cl Ge O1.5 P2
• Title of publication: Synthesis of Zwitterionic Group 14 Centered Complexes: Traditional Coordination and Unusual Insertion Chemistry
• Authors of publication: Weicker, Sarah A.; Dube, Jonathan W.; Ragogna, Paul J.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 22
• Pages of publication: 6681
• a: 16.945 ± 0.003 Å
• b: 17.225 ± 0.003 Å
• c: 26.033 ± 0.005 Å
• α: 90°
• β: 96.49 ± 0.03°
• γ: 90°
• Cell volume: 7550 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0606
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for significantly intense reflections: 0.101
• Weighted residual factors for all reflections included in the refinement: 0.1106
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No