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Information card for entry 4081790
Preview
Coordinates | 4081790.cif |
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Original paper (by DOI) | HTML |
Formula | C35 H62 Ga Ge N3 S |
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Calculated formula | C35 H62 Ga Ge N3 S |
SMILES | [Ge]1(C(=C\C(C)(C)C)/[Ga](C(C)(C)C)(C(C)(C)C)[S]=C(N1c1ccccc1)N(CC)CC)(C#CC(C)(C)C)N(CC)CC |
Title of publication | Cooperative Ge‒N Bond Activation in Hydrogallation Products of Alkynyl(diethylamino)germanes (Et2N)nGe(C≡CtBu)4‒n |
Authors of publication | Uhl, Werner; Tannert, Jens; Layh, Marcus; Hepp, Alexander; Grimme, Stefan; Risthaus, Tobias |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 22 |
Pages of publication | 6770 |
a | 11.2381 ± 0.0006 Å |
b | 21.1647 ± 0.0011 Å |
c | 16.3711 ± 0.0008 Å |
α | 90° |
β | 92.162 ± 0.001° |
γ | 90° |
Cell volume | 3891.1 ± 0.3 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0267 |
Residual factor for significantly intense reflections | 0.0232 |
Weighted residual factors for significantly intense reflections | 0.0603 |
Weighted residual factors for all reflections included in the refinement | 0.0622 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.047 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4081790.html
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