Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4081794
Preview
Coordinates | 4081794.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Tip2Si=SiTipTMOP |
---|---|
Chemical name | 1,1,2-Tris(2,4,6-triisopropylphenyl)-2-(2,4,6-trimethoxyphenyl)disilene |
Formula | C54 H80 O3 Si2 |
Calculated formula | C54 H80 O3 Si2 |
Title of publication | Potential Protecting Group Strategy for Disila Analogues of Vinyllithiums: Synthesis and Reactivity of a 2,4,6-Trimethoxyphenyl-Substituted Disilene |
Authors of publication | Meltzer, Antje; Majumdar, Moumita; White, Andrew J. P.; Huch, Volker; Scheschkewitz, David |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 22 |
Pages of publication | 6844 |
a | 13.4402 ± 0.0004 Å |
b | 14.0958 ± 0.0006 Å |
c | 15.3783 ± 0.0005 Å |
α | 93.628 ± 0.003° |
β | 100.148 ± 0.003° |
γ | 115.006 ± 0.003° |
Cell volume | 2567.85 ± 0.18 Å3 |
Cell temperature | 173 K |
Ambient diffraction temperature | 173 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0679 |
Residual factor for significantly intense reflections | 0.051 |
Weighted residual factors for significantly intense reflections | 0.132 |
Weighted residual factors for all reflections included in the refinement | 0.1438 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.035 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4081794.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.