Information card for entry 4081806

Structure parameters

• Formula: C65.33 H81.74 Al1.33 N4 O2
• Calculated formula: C65.3333 H81.7333 Al1.33333 N4 O2
• Title of publication: Aluminum‒Amido-Mediated Heterolytic Addition of Water Affords an Alumoxane
• Authors of publication: Myers, Thomas W.; Berben, Louise A.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 22
• Pages of publication: 6647
• a: 14.9583 ± 0.0003 Å
• b: 26.8456 ± 0.0005 Å
• c: 22.0759 ± 0.0004 Å
• α: 90°
• β: 107.032 ± 0.001°
• γ: 90°
• Cell volume: 8476.1 ± 0.3 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0824
• Residual factor for significantly intense reflections: 0.0632
• Weighted residual factors for significantly intense reflections: 0.1724
• Weighted residual factors for all reflections included in the refinement: 0.1887
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No