Crystallography Open Database

Information card for entry 4081894

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Coordinates	4081894.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H31 Au O9 Os3 P
Calculated formula	C46 H31 Au O9 Os3 P
Title of publication	Unsaturated Triosmium Carbonyl Cluster Complexes with Bridging Aryl Ligands: Structures, Bonding, and Transformations
Authors of publication	Adams, Richard D.; Rassolov, Vitaly; Zhang, Qiang
Journal of publication	Organometallics
Year of publication	2013
Journal volume	32
Journal issue	21
Pages of publication	6368
a	9.8364 ± 0.0003 Å
b	12.6236 ± 0.0003 Å
c	19.9043 ± 0.0005 Å
α	94.96 ± 0.001°
β	103.5 ± 0.001°
γ	111.308 ± 0.001°
Cell volume	2198.57 ± 0.1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0362
Residual factor for significantly intense reflections	0.0296
Weighted residual factors for significantly intense reflections	0.0829
Weighted residual factors for all reflections included in the refinement	0.0918
Goodness-of-fit parameter for all reflections included in the refinement	1.021
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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