Information card for entry 4081988

Structure parameters

• Formula: C40 H64 N4 O3 Si2 Yb
• Calculated formula: C40 H64 N4 O3 Si2 Yb
• Title of publication: Unusual Redox Chemistry of Ytterbium Carbazole‒Bis(oxazoline) Compounds: Oxidative Coupling of Primary Phosphines by an Ytterbium Carbazole‒Bis(oxazoline) Dialkyl
• Authors of publication: Zou, Jin; Berg, David J.; Oliver, Allen; Twamley, Brendan
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 21
• Pages of publication: 6532
• a: 11.0731 ± 0.0011 Å
• b: 20.486 ± 0.002 Å
• c: 19.0196 ± 0.0019 Å
• α: 90°
• β: 96.291 ± 0.002°
• γ: 90°
• Cell volume: 4288.5 ± 0.7 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0179
• Residual factor for significantly intense reflections: 0.0148
• Weighted residual factors for significantly intense reflections: 0.0357
• Weighted residual factors for all reflections included in the refinement: 0.037
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No