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Information card for entry 4081993
Preview
Coordinates | 4081993.cif |
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Original paper (by DOI) | HTML |
Formula | C27 H49 Cl N O P2 Rh |
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Calculated formula | C27 H49 Cl N O P2 Rh |
SMILES | C1c2c3c(cc(c2C[P](C(C)(C)C)(C(C)(C)C)[Rh]1(N=O)([P](C3)(C(C)(C)C)C(C)(C)C)Cl)C)C |
Title of publication | Electron Transfer Behavior of Pincer-Type {RhNO}8Complexes: Spectroscopic Characterization and Reactivity of Paramagnetic {RhNO}9Complexes |
Authors of publication | Pellegrino, Juan; Gaviglio, Carina; Milstein, David; Doctorovich, Fabio |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 21 |
Pages of publication | 6555 |
a | 10.4103 ± 0.0004 Å |
b | 23.045 ± 0.0007 Å |
c | 12.0078 ± 0.0004 Å |
α | 90° |
β | 94.001 ± 0.003° |
γ | 90° |
Cell volume | 2873.71 ± 0.17 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.062 |
Residual factor for significantly intense reflections | 0.0531 |
Weighted residual factors for significantly intense reflections | 0.1252 |
Weighted residual factors for all reflections included in the refinement | 0.1322 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.044 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4081993.html
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