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Information card for entry 4082115
Preview
Coordinates | 4082115.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C31 H37 Cl2 F3 N2 O3 Os S |
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Calculated formula | C31 H37 Cl2 F3 N2 O3 Os S |
Title of publication | Synthesis, Characterization, and Reactivity of the First Osmium β-Diketiminato Complexes and Application in Catalysis |
Authors of publication | Schreiber, Dominique F.; O’Connor, Crystal; Grave, Christian; Müller-Bunz, Helge; Scopelliti, Rosario; Dyson, Paul J.; Phillips, Andrew D. |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 24 |
Pages of publication | 7345 |
a | 12.2652 ± 0.0003 Å |
b | 11.857 ± 0.0002 Å |
c | 21.7502 ± 0.0004 Å |
α | 90° |
β | 94.327 ± 0.002° |
γ | 90° |
Cell volume | 3154.08 ± 0.11 Å3 |
Cell temperature | 133 ± 2 K |
Ambient diffraction temperature | 133 ± 2 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0214 |
Residual factor for significantly intense reflections | 0.0188 |
Weighted residual factors for significantly intense reflections | 0.0462 |
Weighted residual factors for all reflections included in the refinement | 0.0469 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4082115.html
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