Crystallography Open Database

Information card for entry 4082217

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Coordinates	4082217.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H72 N4 O12 Os3 Pd2
Calculated formula	C66 H72 N4 O12 Os3 Pd2
Title of publication	Palladium‒Osmium Heterometallic Clusters Containing N-Heterocyclic Carbene Ligands
Authors of publication	Liu, Yu; Ganguly, Rakesh; Huynh, Han Vinh; Leong, Weng Kee
Journal of publication	Organometallics
Year of publication	2013
Journal volume	32
Journal issue	24
Pages of publication	7559
a	19.8497 ± 0.0009 Å
b	20.6112 ± 0.0009 Å
c	33.6302 ± 0.0016 Å
α	90°
β	90°
γ	90°
Cell volume	13759 ± 1.1 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	6
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0701
Residual factor for significantly intense reflections	0.0456
Weighted residual factors for significantly intense reflections	0.1057
Weighted residual factors for all reflections included in the refinement	0.128
Goodness-of-fit parameter for all reflections included in the refinement	1.101
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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