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Information card for entry 4082226
Preview
Coordinates | 4082226.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C54 H50 Cl2 F3 N3 O10 Pd S |
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Calculated formula | C54 H46 Cl2 F3 N3 O10 Pd S |
Title of publication | Insertion Reactions of Six-Membered CyclopalladatedN,N′,N″-Triarylguanidine, [Pd{κ2(C,N)-C6H3Me-3(NHC(NHAr)(═NAr))-2}(μ-Br)]2(Ar = 2-MeC6H4) with PhC≡C—C(O)OR (R = Me and Et): A Gateway to Second Orthopalladation through Novel Rearrangements |
Authors of publication | Saxena, Priya; Thirupathi, Natesan; Nethaji, Munirathinam |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 24 |
Pages of publication | 7580 |
a | 13.5054 ± 0.0005 Å |
b | 14.2285 ± 0.0005 Å |
c | 28.8166 ± 0.0014 Å |
α | 90° |
β | 92.806 ± 0.004° |
γ | 90° |
Cell volume | 5530.8 ± 0.4 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0794 |
Residual factor for significantly intense reflections | 0.074 |
Weighted residual factors for significantly intense reflections | 0.2002 |
Weighted residual factors for all reflections included in the refinement | 0.2045 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.1 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4082226.html
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