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Information card for entry 4082248
Preview
Coordinates | 4082248.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C35 H35 Cl2 N P2 Pd |
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Calculated formula | C35 H35 Cl2 N P2 Pd |
SMILES | [Pd]1([P](c2c(P(=[N]1[C@@H](C)C(C)C)(c1ccccc1)c1ccccc1)cccc2)(c1ccccc1)c1ccccc1)(Cl)Cl |
Title of publication | Nitrogen-Assisted Ortho Lithiation: One-Pot Synthesis of New Classes of Bidentate and Tetradentate Mixed Pσim N Ligands |
Authors of publication | Boubekeur, Leila; Ricard, Louis; Mézailles, Nicolas; Demange, Matthieu; Auffrant, Audrey; Le Floch, Pascal |
Journal of publication | Organometallics |
Year of publication | 2006 |
Journal volume | 25 |
Journal issue | 12 |
Pages of publication | 3091 |
a | 8.495 ± 0.001 Å |
b | 16.87 ± 0.001 Å |
c | 11.447 ± 0.001 Å |
α | 90° |
β | 106.974 ± 0.001° |
γ | 90° |
Cell volume | 1569 ± 0.2 Å3 |
Cell temperature | 150 ± 0.1 K |
Ambient diffraction temperature | 150 ± 0.1 K |
Number of distinct elements | 6 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0197 |
Residual factor for significantly intense reflections | 0.0191 |
Weighted residual factors for significantly intense reflections | 0.0517 |
Weighted residual factors for all reflections included in the refinement | 0.0522 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.007 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4082248.html
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