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Information card for entry 4082265
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Coordinates | 4082265.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | [(η^5^-C~5~Me~5~)Ru{=C(-OC~6~H~3~OH-CH(C~6~H~4~F)CH~2~-)}(dippe)][BF~4~] |
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Chemical name | 1,2-bis(diisopropylphosphine)ethane-7-hydroxy-4-p-fluorphenyl-chroman-2- ylidene-η^5^-pentamethylcyclopentadienyl-ruthenium (II) tetrafluorborate |
Formula | C39 H57 B F5 O2 P2 Ru |
Calculated formula | C39 H58 B F5 O2 P2 Ru |
Title of publication | γ-Substituted Vinylidene, Chroman-2-ylidene, and Hexahydrochromen-2-ylidene from Ruthenium Allenylidene/Alkenylcarbyne Complexes |
Authors of publication | Bustelo, Emilio; Jiménez-Tenorio, Manuel; Puerta, M. Carmen; Valerga, Pedro |
Journal of publication | Organometallics |
Year of publication | 2007 |
Journal volume | 26 |
Journal issue | 17 |
Pages of publication | 4300 |
a | 10.68 ± 0.002 Å |
b | 10.981 ± 0.002 Å |
c | 17.341 ± 0.004 Å |
α | 93.24 ± 0.03° |
β | 92.81 ± 0.03° |
γ | 105.96 ± 0.03° |
Cell volume | 1947.8 ± 0.7 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0782 |
Residual factor for significantly intense reflections | 0.0737 |
Weighted residual factors for significantly intense reflections | 0.1483 |
Weighted residual factors for all reflections included in the refinement | 0.151 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.064 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4082265.html
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Users of the data should acknowledge the original authors of the
structural data.