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Information card for entry 4082377
Preview
Coordinates | 4082377.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C25.5 H28.5 Cl5.5 Co N3 O7 |
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Calculated formula | C25.5 H28.5 Cl5.5 Co N3 O7 |
Title of publication | A Novel Series of CoIII(salen-type) Complexes Containing a Seven-Membered Metallacycle: Synthesis, Structural Characterization and Factors Affecting the Metallacyclization Rate |
Authors of publication | Siega, Patrizia; Dreos, Renata; Brancatelli, Giovanna; Zangrando, Ennio; Tavagnacco, Claudio; Vrdoljak, Višnja; Hrenar, Tomica |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 4 |
Pages of publication | 909 |
a | 19.993 ± 0.003 Å |
b | 12.989 ± 0.003 Å |
c | 24.117 ± 0.003 Å |
α | 90° |
β | 94.69 ± 0.03° |
γ | 90° |
Cell volume | 6242 ± 1.9 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0958 |
Residual factor for significantly intense reflections | 0.067 |
Weighted residual factors for significantly intense reflections | 0.1759 |
Weighted residual factors for all reflections included in the refinement | 0.1973 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.02 |
Diffraction radiation wavelength | 1.5418 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4082377.html
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