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Information card for entry 4082384
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Coordinates | 4082384.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C15 H22 O4 Si |
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Calculated formula | C15 H22 O4 Si |
Title of publication | Synthesis of 4-Silacyclohexan-1-ones and (4-Silacyclohexan-1-yl)amines Containing the Silicon Protecting Groups MOP (4-Methoxyphenyl), DMOP (2,4-Dimethoxyphenyl), or TMOP (2,4,6-Trimethoxyphenyl): Versatile Si- and C-Functional Building Blocks for Synthesis |
Authors of publication | Fischer, Markus; Burschka, Christian; Tacke, Reinhold |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 4 |
Pages of publication | 1020 |
a | 17.367 ± 0.003 Å |
b | 10.079 ± 0.0012 Å |
c | 19.795 ± 0.003 Å |
α | 90° |
β | 113.619 ± 0.016° |
γ | 90° |
Cell volume | 3174.7 ± 0.9 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 4 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0523 |
Residual factor for significantly intense reflections | 0.041 |
Weighted residual factors for significantly intense reflections | 0.1087 |
Weighted residual factors for all reflections included in the refinement | 0.1149 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.063 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4082384.html
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