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Information card for entry 4082386
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Coordinates | 4082386.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C20 H24 O4 Si |
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Calculated formula | C20 H24 O4 Si |
SMILES | C1CC(=O)CC[Si]1(c1c(cc(cc1OC)OC)OC)c1ccccc1 |
Title of publication | Synthesis of 4-Silacyclohexan-1-ones and (4-Silacyclohexan-1-yl)amines Containing the Silicon Protecting Groups MOP (4-Methoxyphenyl), DMOP (2,4-Dimethoxyphenyl), or TMOP (2,4,6-Trimethoxyphenyl): Versatile Si- and C-Functional Building Blocks for Synthesis |
Authors of publication | Fischer, Markus; Burschka, Christian; Tacke, Reinhold |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 4 |
Pages of publication | 1020 |
a | 9.3403 ± 0.0019 Å |
b | 23.911 ± 0.005 Å |
c | 8.7619 ± 0.0018 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1956.8 ± 0.7 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 4 |
Space group number | 33 |
Hermann-Mauguin space group symbol | P n a 21 |
Hall space group symbol | P 2c -2n |
Residual factor for all reflections | 0.044 |
Residual factor for significantly intense reflections | 0.0364 |
Weighted residual factors for significantly intense reflections | 0.0901 |
Weighted residual factors for all reflections included in the refinement | 0.095 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.049 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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