Information card for entry 4082398

Structure parameters

• Formula: C55 H70 Cl6 N6 V2
• Calculated formula: C55 H58 Cl6 N6 V2
• Title of publication: Synthesis of (Imido)vanadium(V) Complexes Containing 8-(2,6-Dimethylanilide)-5,6,7-trihydroquinoline Ligands: Highly Active Catalyst Precursors for Ethylene Dimerization
• Authors of publication: Tang, Xiao-Yan; Igarashi, Atsushi; Sun, Wen-Hua; Inagaki, Akiko; Liu, Jingyu; Zhang, Wenjuan; Li, Yue-Sheng; Nomura, Kotohiro
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 4
• Pages of publication: 1053
• a: 32.189 ± 0.005 Å
• b: 10.1323 ± 0.0016 Å
• c: 16.883 ± 0.003 Å
• α: 90°
• β: 104.38 ± 0.006°
• γ: 90°
• Cell volume: 5333.9 ± 1.5 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0771
• Residual factor for significantly intense reflections: 0.057
• Weighted residual factors for significantly intense reflections: 0.1442
• Weighted residual factors for all reflections included in the refinement: 0.166
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No