Crystallography Open Database

Information card for entry 4082492

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Coordinates	4082492.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C59 H52 Cl N2 P3 Rh Si
Calculated formula	C59 H52 Cl N2 P3 Rh Si
Title of publication	N-Heterocyclic Silyl Pincer Ligands
Authors of publication	Dixon, Lily S. H.; Hill, Anthony F.; Sinha, Arup; Ward, Jas S.
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	3
Pages of publication	653
a	11.7435 ± 0.0001 Å
b	13.3987 ± 0.0002 Å
c	17.0566 ± 0.0002 Å
α	87.2376 ± 0.0007°
β	86.4154 ± 0.0008°
γ	67.1037 ± 0.0006°
Cell volume	2466.69 ± 0.05 Å³
Cell temperature	200 K
Ambient diffraction temperature	200 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0445
Residual factor for significantly intense reflections	0.0341
Weighted residual factors for all reflections	0.084
Weighted residual factors for significantly intense reflections	0.079
Weighted residual factors for all reflections included in the refinement	0.084
Goodness-of-fit parameter for all reflections included in the refinement	0.9812
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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