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Information card for entry 4082498
Preview
Coordinates | 4082498.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H46 Cl2 P2 Pd |
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Calculated formula | C24 H46 Cl2 P2 Pd |
SMILES | [Pd]([P]1(C2CCCC1CCC2)CCCC)([P]1(C2CCCC1CCC2)CCCC)(Cl)Cl |
Title of publication | Unexpectedly High Barriers to M‒P Rotation in Tertiary Phobane Complexes: PhobPR Behavior That Is Commensurate withtBu2PR |
Authors of publication | Lister, Julia M.; Carreira, Monica; Haddow, Mairi F.; Hamilton, Alex; McMullin, Claire L.; Orpen, A. Guy; Pringle, Paul G.; Stennett, Tom E. |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 3 |
Pages of publication | 702 |
a | 7.765 ± 0.0003 Å |
b | 7.8175 ± 0.0004 Å |
c | 11.0564 ± 0.0005 Å |
α | 97.289 ± 0.003° |
β | 103.064 ± 0.003° |
γ | 96.625 ± 0.003° |
Cell volume | 641.25 ± 0.05 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0604 |
Residual factor for significantly intense reflections | 0.0556 |
Weighted residual factors for significantly intense reflections | 0.1441 |
Weighted residual factors for all reflections included in the refinement | 0.1467 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.121 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4082498.html
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