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Information card for entry 4082538
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Coordinates | 4082538.cif |
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Original paper (by DOI) | HTML |
Formula | C44 H43 Cl5 N P Pd |
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Calculated formula | C44 H43 Cl5 N P Pd |
Title of publication | Reactivity toward Neutral N- and P-Donor Ligands of Eight-Membered Palladacycles Arising from Monoinsertion of Alkynes into the Pd‒C Bond of Orthopalladated Homoveratrylamine and Phentermine. A New Example of the Transphobia Effect |
Authors of publication | Oliva-Madrid, María-José; García-López, José-Antonio; Saura-Llamas, Isabel; Bautista, Delia; Vicente, José |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 1 |
Pages of publication | 33 |
a | 10.92 ± 0.0008 Å |
b | 14.2254 ± 0.0012 Å |
c | 14.675 ± 0.0011 Å |
α | 72.231 ± 0.002° |
β | 70.129 ± 0.002° |
γ | 81.274 ± 0.002° |
Cell volume | 2038.7 ± 0.3 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0263 |
Residual factor for significantly intense reflections | 0.025 |
Weighted residual factors for significantly intense reflections | 0.0608 |
Weighted residual factors for all reflections included in the refinement | 0.0616 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.055 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4082538.html
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