Information card for entry 4082568

Structure parameters

• Formula: C24 H45 Cu F3 N5 O3 S Si
• Calculated formula: C24 H45 Cu F3 N5 O3 S Si
• Title of publication: Facile Access to Mono- and Dinuclear Heteroleptic N-Heterocyclic Silylene Copper Complexes
• Authors of publication: Tan, Gengwen; Blom, Burgert; Gallego, Daniel; Driess, Matthias
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 1
• Pages of publication: 363
• a: 10.0327 ± 0.0008 Å
• b: 30.6715 ± 0.0015 Å
• c: 10.8305 ± 0.0007 Å
• α: 90°
• β: 106.542 ± 0.007°
• γ: 90°
• Cell volume: 3194.8 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1079
• Residual factor for significantly intense reflections: 0.0707
• Weighted residual factors for significantly intense reflections: 0.1148
• Weighted residual factors for all reflections included in the refinement: 0.1263
• Goodness-of-fit parameter for all reflections included in the refinement: 1.126
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No