Information card for entry 4082756

Structure parameters

• Formula: C51 H73 O2 P2 Rh
• Calculated formula: C51 H73 O2 P2 Rh
• Title of publication: Synthesis of a Rhodium Carbonyl Phosphaalkenyl‒Phosphido Complex: A Phosphorus Congener of Schiff Base Type N,N′-Chelating Monoanionic Ligands
• Authors of publication: Matsumoto, Teruyuki; Sasamori, Takahiro; Miyake, Hideaki; Tokitoh, Norihiro
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 6
• Pages of publication: 1341
• a: 9.6326 ± 0.0002 Å
• b: 15.266 ± 0.0004 Å
• c: 18.9224 ± 0.0006 Å
• α: 111.911 ± 0.0012°
• β: 93.5674 ± 0.0012°
• γ: 106.429 ± 0.0016°
• Cell volume: 2431.76 ± 0.12 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0648
• Residual factor for significantly intense reflections: 0.0383
• Weighted residual factors for significantly intense reflections: 0.0723
• Weighted residual factors for all reflections included in the refinement: 0.0777
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No