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Information card for entry 4082782
Preview
Coordinates | 4082782.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C176 H176 F24 N16 O42 Rh4 S8 Zn2 |
---|---|
Calculated formula | C164 H132 F24 N16 O32 Rh4 S8 Zn2 |
SMILES | c12c3c4c5ccccc5c5O[Rh]6789(Oc(c35)c3ccccc23)([c]2([c]9([c]8([c]7([c]62C)C)C)C)C)[n]2ccc(c3cc5[n]6c(c3)c3[n](cccc3)[Zn]376([n]6ccccc6c6[n]3c(cc(c6)c3cc[n](cc3)[Rh]3689%10(Oc%11c%12c(c%13ccccc%13c%13O[Rh]%14%15%16%17(Oc(c%12%13)c%12ccccc%11%12)([n]%11ccc(c%12cc%13[n]%18c(c%12)c%12[n](cccc%12)[Zn]%12%19%18([n]%18ccccc%18c%18[n]%12c(cc(c%18)c%12cc[n](cc%12)[Rh]%12%18%20%21(O1)(O4)[c]1([c]%12([c]%18([c]%20([c]%211C)C)C)C)C)c1[n]%19cccc1)[n]1ccccc%131)cc%11)[c]1([c]%17([c]%16([c]%15([c]%141C)C)C)C)C)O3)[c]1([c]6([c]8([c]9([c]%101C)C)C)C)C)c1[n]7cccc1)[n]1ccccc51)cc2.FC(F)(F)S(=O)(=O)[O-].FC(F)(F)S(=O)(=O)[O-].[O-]S(=O)(=O)C(F)(F)F.S(=O)(=O)(C(F)(F)F)[O-].FC(F)(F)S(=O)(=O)[O-].FC(F)(F)S(=O)(=O)[O-].FC(F)(F)S(=O)(=O)[O-].S(=O)(=O)(C(F)(F)F)[O-] |
Title of publication | Box-like Heterometallic Macrocycles Derived from Bis-Terpyridine Metalloligands |
Authors of publication | Liu, Jing-Jing; Lin, Yue-Jian; Jin, Guo-Xin |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 5 |
Pages of publication | 1283 |
a | 16.1642 ± 0.0018 Å |
b | 29.018 ± 0.003 Å |
c | 20.852 ± 0.002 Å |
α | 90° |
β | 102.507 ± 0.002° |
γ | 90° |
Cell volume | 9548.6 ± 1.7 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1238 |
Residual factor for significantly intense reflections | 0.1131 |
Weighted residual factors for significantly intense reflections | 0.2823 |
Weighted residual factors for all reflections included in the refinement | 0.2889 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.086 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4082782.html
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