Information card for entry 4082790

Structure parameters

• Formula: C44 H62 Fe N3 Si
• Calculated formula: C44 H62 Fe N3 Si
• Title of publication: Sequential Reduction and Alkyl Exchange Reactions of Bis(imino)pyridine Dialkyliron(II) with Trimethylaluminum
• Authors of publication: Cartes, M. Ángeles; Rodr\?íguez-Delgado, Antonio; Palma, Pilar; Álvarez, Eleuterio; Cámpora, Juan
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 7
• Pages of publication: 1834
• a: 32.654 ± 0.002 Å
• b: 14.3535 ± 0.001 Å
• c: 9.2139 ± 0.0006 Å
• α: 90°
• β: 105.766 ± 0.001°
• γ: 90°
• Cell volume: 4156.1 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0842
• Residual factor for significantly intense reflections: 0.0503
• Weighted residual factors for significantly intense reflections: 0.1246
• Weighted residual factors for all reflections included in the refinement: 0.1437
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No