Information card for entry 4082827

Structure parameters

• Formula: C119 N10 O22 Ru4 S4
• Calculated formula: C119 N10 O22 Ru4 S4
• Title of publication: Electron-Rich Arene‒Ruthenium Metalla-architectures Incorporating Tetrapyridyl‒Tetrathiafulvene Donor Moieties
• Authors of publication: Vajpayee, Vaishali; Bivaud, Sébastien; Goeb, Sébastien; Croué, Vincent; Allain, Magali; Popp, Brian V.; Garci, Amine; Therrien, Bruno; Sallé, Marc
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 7
• Pages of publication: 1651
• a: 11.281 ± 0.002 Å
• b: 23.941 ± 0.001 Å
• c: 24.096 ± 0.002 Å
• α: 90°
• β: 92.083 ± 0.009°
• γ: 90°
• Cell volume: 6503.5 ± 1.3 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1714
• Residual factor for significantly intense reflections: 0.0886
• Weighted residual factors for significantly intense reflections: 0.2313
• Weighted residual factors for all reflections included in the refinement: 0.318
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No