Information card for entry 4082934

Structure parameters

• Formula: C63 H63 Cl3 Cr N3 O2.5 P4
• Calculated formula: C63 H63 Cl3 Cr N3 O2.5 P4
• Title of publication: Reactivity with Alkylaluminum of a Chromium Complex of a Pyridine-Containing PNP Ligand: Redox N‒P Bond Cleavage
• Authors of publication: Alzamly, Ahmed; Gambarotta, Sandro; Korobkov, Ilia
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 7
• Pages of publication: 1602
• a: 10.3183 ± 0.0004 Å
• b: 12.5463 ± 0.0005 Å
• c: 24.2213 ± 0.001 Å
• α: 86.477 ± 0.002°
• β: 88.342 ± 0.002°
• γ: 73.417 ± 0.002°
• Cell volume: 2999.3 ± 0.2 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0767
• Residual factor for significantly intense reflections: 0.064
• Weighted residual factors for significantly intense reflections: 0.1798
• Weighted residual factors for all reflections included in the refinement: 0.191
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No