Information card for entry 4082940

Structure parameters

• Formula: C71.5 H115 Cl7 N8 O4 S10 Sn6
• Calculated formula: C71.4985 H110 Cl6.997 N8 O4 S10 Sn6
• Title of publication: Diamondoid Hydrazones and Hydrazides: Sterically Demanding Ligands for Sn/S Cluster Design
• Authors of publication: Barth, Beatrix E. K.; Tkachenko, Boryslav A.; Eußner, Jens P.; Schreiner, Peter R.; Dehnen, Stefanie
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 7
• Pages of publication: 1678
• a: 16.2629 ± 0.001 Å
• b: 20.5736 ± 0.0012 Å
• c: 30.064 ± 0.002 Å
• α: 83.694 ± 0.005°
• β: 88.532 ± 0.005°
• γ: 77.329 ± 0.005°
• Cell volume: 9754.6 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1936
• Residual factor for significantly intense reflections: 0.0686
• Weighted residual factors for significantly intense reflections: 0.1072
• Weighted residual factors for all reflections included in the refinement: 0.1376
• Goodness-of-fit parameter for all reflections included in the refinement: 0.804
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No