Information card for entry 4082953

Structure parameters

• Formula: C48 H67 N O3 U
• Calculated formula: C48 H67 N O3 U
• Title of publication: Radical Reductive Elimination from Tetrabenzyluranium Mediated by an Iminoquinone Ligand
• Authors of publication: Matson, Ellen M.; Franke, Sebastian M.; Anderson, Nickolas H.; Cook, Timothy D.; Fanwick, Phillip E.; Bart, Suzanne C.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 8
• Pages of publication: 1964
• a: 11.1583 ± 0.0007 Å
• b: 11.8042 ± 0.0007 Å
• c: 17.5607 ± 0.0013 Å
• α: 77.451 ± 0.006°
• β: 76.928 ± 0.005°
• γ: 87.574 ± 0.004°
• Cell volume: 2199.2 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0533
• Residual factor for significantly intense reflections: 0.0368
• Weighted residual factors for significantly intense reflections: 0.0769
• Weighted residual factors for all reflections included in the refinement: 0.0822
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No