Crystallography Open Database

Information card for entry 4083009

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Coordinates	4083009.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C49 H57 Cl N2 P2 Rh
Calculated formula	C49 H57 Cl N2 P2 Rh
Title of publication	Rh‒FHF and Rh‒F Complexes Containing SmallN-Alkyl Substituted Six-Membered Ring N-Heterocyclic Carbenes
Authors of publication	Bramananthan, Nicola; Carmona, María; Lowe, John P.; Mahon, Mary F.; Poulten, Rebecca C.; Whittlesey, Michael K.
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	8
Pages of publication	1986
a	10.944 ± 0.0001 Å
b	11.705 ± 0.0001 Å
c	18.82 ± 0.0003 Å
α	75.049 ± 0.001°
β	87.841 ± 0.001°
γ	69.93 ± 0.001°
Cell volume	2184.34 ± 0.05 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0472
Residual factor for significantly intense reflections	0.0378
Weighted residual factors for significantly intense reflections	0.0927
Weighted residual factors for all reflections included in the refinement	0.0982
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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