Information card for entry 4083032

Structure parameters

• Formula: C43 H40 F3 O2.5 P2 Pd
• Calculated formula: C43 H35 F2.97 O2.25 P2 Pd
• Title of publication: Direct Access to Fluorene by Successive C–O/C–H Bond Activations of 2-Phenylbenzyl Ester
• Authors of publication: Hirano, Masafumi; Kawazu, Sosuke; Komine, Nobuyuki
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 8
• Pages of publication: 1921
• a: 13.5362 ± 0.0007 Å
• b: 15.1262 ± 0.0006 Å
• c: 18.9707 ± 0.0009 Å
• α: 90°
• β: 93.72 ± 0.003°
• γ: 90°
• Cell volume: 3876.1 ± 0.3 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0738
• Weighted residual factors for all reflections included in the refinement: 0.2091
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No