Information card for entry 4083037

Structure parameters

• Formula: C53 H47 Cl Ni O P2
• Calculated formula: C53 H47 Cl Ni O P2
• Title of publication: A Broadly Applicable Strategy for Entry into Homogeneous Nickel(0) Catalysts from Air-Stable Nickel(II) Complexes.
• Authors of publication: Standley, Eric A.; Smith, Stacey J.; Müller, Peter; Jamison, Timothy F.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 8
• Pages of publication: 2012 - 2018
• a: 11.7668 ± 0.0009 Å
• b: 11.9557 ± 0.0009 Å
• c: 16.0572 ± 0.0012 Å
• α: 82.914 ± 0.002°
• β: 69.186 ± 0.001°
• γ: 83.528 ± 0.002°
• Cell volume: 2089.6 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0275
• Residual factor for significantly intense reflections: 0.0258
• Weighted residual factors for significantly intense reflections: 0.0692
• Weighted residual factors for all reflections included in the refinement: 0.0704
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No