Information card for entry 4083099

Structure parameters

• Formula: C66 H53 B F24 P Rh
• Calculated formula: C66 H53 B F24 P Rh
• Title of publication: Reversibility of 1,4-Metal Migration in Cp*RhIIIand Cp*IrIIIComplexes
• Authors of publication: Ikeda, Yousuke; Takano, Koichi; Waragai, Maiko; Kodama, Shintaro; Tsuchida, Noriko; Takano, Keiko; Ishii, Youichi
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 9
• Pages of publication: 2142
• a: 13.065 ± 0.003 Å
• b: 13.86 ± 0.003 Å
• c: 34.505 ± 0.007 Å
• α: 90°
• β: 95.303 ± 0.003°
• γ: 90°
• Cell volume: 6221 ± 2 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0887
• Weighted residual factors for all reflections included in the refinement: 0.2315
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No