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Information card for entry 4083130
Preview
Coordinates | 4083130.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C84 H92 N8 O11 P2 Te5 |
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Calculated formula | C84 H92 N8 O11 P2 Te5 |
SMILES | [Te]123(O[Te]4(c5ccccc5N=Nc5ccccc5)O[Te]([O]=P(O[Te](c5ccccc5N=Nc5ccccc5)(O2)O[Te](OP(=[O]4)(C2CCCCC2)C2CCCCC2)(O3)c2c(N=Nc3ccccc3)cccc2)(C2CCCCC2)C2CCCCC2)(O1)c1c(N=Nc2ccccc2)cccc1)=O.c1ccccc1.c1ccccc1 |
Title of publication | Reactions of RTeCl3(R = 2-phenylazophenyl) with Diorganophosphinic Acids. Te‒C Bond Cleavage and Stabilization of the Te═O Motif in an Umbrella-Shaped Te5O11P2Multi-metallacyclic Framework |
Authors of publication | Metre, Ramesh K.; Kundu, Subrata; Sahoo, Dipankar; Chandrasekhar, Vadapalli |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 9 |
Pages of publication | 2380 |
a | 10.852 ± 0.005 Å |
b | 19.673 ± 0.005 Å |
c | 20.666 ± 0.005 Å |
α | 82.173 ± 0.005° |
β | 74.833 ± 0.005° |
γ | 73.995 ± 0.005° |
Cell volume | 4084 ± 2 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0933 |
Residual factor for significantly intense reflections | 0.0592 |
Weighted residual factors for significantly intense reflections | 0.1439 |
Weighted residual factors for all reflections included in the refinement | 0.1618 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.049 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4083130.html
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Users of the data should acknowledge the original authors of the
structural data.