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Information card for entry 4083207
Preview
Coordinates | 4083207.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H20 N8 Si |
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Calculated formula | C28 H20 N8 Si |
SMILES | [Si](n1ccc2cccnc12)(n1ccc2cccnc12)(n1ccc2cccnc12)n1ccc2cccnc12 |
Title of publication | 7-Azaindol-1-yl(organo)silanes and Their PdCl2Complexes: Pd-Capped Tetrahedral Silicon Coordination Spheres and Paddlewheels with a Pd‒Si Axis |
Authors of publication | Wahlicht, Sven; Brendler, Erica; Heine, Thomas; Zhechkov, Lyuben; Wagler, Jörg |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 10 |
Pages of publication | 2479 |
a | 9.3497 ± 0.0008 Å |
b | 11.6084 ± 0.001 Å |
c | 12.2956 ± 0.001 Å |
α | 82.554 ± 0.007° |
β | 73.025 ± 0.007° |
γ | 71.534 ± 0.007° |
Cell volume | 1209.63 ± 0.19 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0604 |
Residual factor for significantly intense reflections | 0.0377 |
Weighted residual factors for significantly intense reflections | 0.0825 |
Weighted residual factors for all reflections included in the refinement | 0.0905 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.036 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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