Crystallography Open Database

Information card for entry 4083530

Preview

Coordinates	4083530.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H62 B2 Li2 O8 P2
Calculated formula	C34 H62 B2 Li2 O8 P2
Title of publication	Synthesis and Reactivity ofo-Phosphane Oxide Substituted Aryl(hydro)borates and Aryl(hydro)boranes
Authors of publication	Breunig, Jens Michael; Lehmann, Felix; Bolte, Michael; Lerner, Hans-Wolfram; Wagner, Matthias
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	12
Pages of publication	3163
a	11.6441 ± 0.0014 Å
b	11.3912 ± 0.0008 Å
c	15.7074 ± 0.0018 Å
α	90°
β	100.691 ± 0.009°
γ	90°
Cell volume	2047.3 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0801
Residual factor for significantly intense reflections	0.0646
Weighted residual factors for significantly intense reflections	0.1573
Weighted residual factors for all reflections included in the refinement	0.1654
Goodness-of-fit parameter for all reflections included in the refinement	1.095
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4083530.html