Crystallography Open Database

Information card for entry 4083542

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Coordinates	4083542.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C112 H184 B4 Li4 O8 P8
Calculated formula	C112 H184 B4 Li4 O8 P8
Title of publication	Synthesis and Reactivity ofo-Phosphane Oxide Substituted Aryl(hydro)borates and Aryl(hydro)boranes
Authors of publication	Breunig, Jens Michael; Lehmann, Felix; Bolte, Michael; Lerner, Hans-Wolfram; Wagner, Matthias
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	12
Pages of publication	3163
a	11.822 ± 0.002 Å
b	13.84 ± 0.002 Å
c	19.008 ± 0.003 Å
α	77.506 ± 0.012°
β	87.659 ± 0.014°
γ	76.638 ± 0.012°
Cell volume	2954 ± 0.8 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1862
Residual factor for significantly intense reflections	0.0629
Weighted residual factors for significantly intense reflections	0.0939
Weighted residual factors for all reflections included in the refinement	0.1308
Goodness-of-fit parameter for all reflections included in the refinement	0.73
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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