Information card for entry 4083801

Structure parameters

• Formula: C21 H19 Cl3 N2 O6 Rh2
• Calculated formula: C21 H19 Cl3 N2 O6 Rh2
• Title of publication: Axial Interaction of the [Ru2(CO)4]2+Core with the Aryl C−H Bond: Route to Cyclometalated Compounds Involving a Metal−Metal-Bonded Diruthenium Unit
• Authors of publication: Patra, Sanjib K.; Bera, Jitendra K.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 26
• Pages of publication: 6054
• a: 16.2584 ± 0.0008 Å
• b: 8.3 ± 0.0004 Å
• c: 19.3585 ± 0.001 Å
• α: 90°
• β: 109.431 ± 0.001°
• γ: 90°
• Cell volume: 2463.5 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0386
• Residual factor for significantly intense reflections: 0.0355
• Weighted residual factors for significantly intense reflections: 0.0928
• Weighted residual factors for all reflections included in the refinement: 0.0949
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No