Information card for entry 4083903

Structure parameters

• Formula: C59 H43 Cl9 N5 O Rh
• Calculated formula: C56 H40 N5 O Rh
• Title of publication: Alkylation of Rhodium Porphyrins Using Ammonium and Quinolinium Salts
• Authors of publication: Thompson, Samuel J.; Dong, Guangbin
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 14
• Pages of publication: 3757
• a: 13.067 ± 0.002 Å
• b: 27.509 ± 0.005 Å
• c: 15.892 ± 0.003 Å
• α: 90°
• β: 113.055 ± 0.004°
• γ: 90°
• Cell volume: 5256.3 ± 1.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0852
• Residual factor for significantly intense reflections: 0.0577
• Weighted residual factors for significantly intense reflections: 0.1374
• Weighted residual factors for all reflections included in the refinement: 0.1439
• Goodness-of-fit parameter for all reflections included in the refinement: 1.242
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No