Information card for entry 4083906

Structure parameters

• Formula: C46.5 H33 Cl2 N4 Rh
• Calculated formula: C46.5 H33 Cl2 N4 Rh
• Title of publication: Alkylation of Rhodium Porphyrins Using Ammonium and Quinolinium Salts
• Authors of publication: Thompson, Samuel J.; Dong, Guangbin
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 14
• Pages of publication: 3757
• a: 11.235 ± 0.0008 Å
• b: 13.1958 ± 0.001 Å
• c: 13.8948 ± 0.001 Å
• α: 104.215 ± 0.002°
• β: 107.305 ± 0.002°
• γ: 99.963 ± 0.002°
• Cell volume: 1837.9 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0825
• Residual factor for significantly intense reflections: 0.0597
• Weighted residual factors for significantly intense reflections: 0.1084
• Weighted residual factors for all reflections included in the refinement: 0.1178
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No