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Information card for entry 4084012
Preview
Coordinates | 4084012.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H10 Cl O10 Os3 Sb |
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Calculated formula | C22 H10 Cl O10 Os3 Sb |
SMILES | [Os]12([Os]([Os]([Sb]1(c1ccccc1)c1ccccc1)(C#[O])(C#[O])(C#[O])[Cl]2)(C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O] |
Title of publication | Binuclear Oxidative Addition of Sb‒Cl Bonds: A Facile Synthetic Route to Main Group‒Transition Element Clusters and Rings |
Authors of publication | Li, Ying-Zhou; Ganguly, Rakesh; Leong, Weng Kee |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 14 |
Pages of publication | 3867 |
a | 9.1927 ± 0.0008 Å |
b | 12.0103 ± 0.0008 Å |
c | 12.4195 ± 0.0009 Å |
α | 82.944 ± 0.003° |
β | 84.716 ± 0.002° |
γ | 84.485 ± 0.002° |
Cell volume | 1350.04 ± 0.18 Å3 |
Cell temperature | 103 ± 2 K |
Ambient diffraction temperature | 103 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0275 |
Residual factor for significantly intense reflections | 0.0235 |
Weighted residual factors for significantly intense reflections | 0.0646 |
Weighted residual factors for all reflections included in the refinement | 0.0839 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.294 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4084012.html
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Users of the data should acknowledge the original authors of the
structural data.