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Information card for entry 4084016
Preview
Coordinates | 4084016.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C34.9 H21.8 Cl3.8 O10 Os3 Sb2 |
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Calculated formula | C34.9 H21.8 Cl3.8 O10 Os3 Sb2 |
Title of publication | Binuclear Oxidative Addition of Sb‒Cl Bonds: A Facile Synthetic Route to Main Group‒Transition Element Clusters and Rings |
Authors of publication | Li, Ying-Zhou; Ganguly, Rakesh; Leong, Weng Kee |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 14 |
Pages of publication | 3867 |
a | 11.5786 ± 0.0005 Å |
b | 14.0291 ± 0.0006 Å |
c | 14.9583 ± 0.0006 Å |
α | 102.033 ± 0.002° |
β | 101.686 ± 0.002° |
γ | 106.124 ± 0.002° |
Cell volume | 2193.46 ± 0.17 Å3 |
Cell temperature | 103 ± 2 K |
Ambient diffraction temperature | 103 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0686 |
Residual factor for significantly intense reflections | 0.0535 |
Weighted residual factors for significantly intense reflections | 0.1274 |
Weighted residual factors for all reflections included in the refinement | 0.1365 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.131 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4084016.html
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Users of the data should acknowledge the original authors of the
structural data.